Crystal structure of tetrakisdiphenylammonium hexadecachlorotetrabismuthate(III)
Identifieur interne : 001D57 ( Main/Exploration ); précédent : 001D56; suivant : 001D58Crystal structure of tetrakisdiphenylammonium hexadecachlorotetrabismuthate(III)
Auteurs : Khalid A. Al-Farhan [Arabie saoudite] ; Abdulaziz I. Al-Wassil [Arabie saoudite]Source :
- Journal of Chemical Crystallography [ 1074-1542 ] ; 1995-12-01.
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Abstract
Abstract: [(C6H5)2NH2]4 +[Bi4Cl16]4− crystallizes in the triclinic space group $$P\bar 1$$ witha=11.835(2),b=12.393(2),c=12.625(3)Å, α=108.37(3), β=108.69(3), γ=96.00(3)° andD c=2.135 g cm−3 forZ=1. The [Bi4Cl16]4− anion is a centrosymmetric cluster of four distorted edge-sharing BiCl6 octahedra. The ranges of the Bi−Cl bonds are 2.484(4)–2.606(3)Å for Bi−Cl(terminal), 2.691(3)–2.956(4)Å for Bi-Cl(µ2), and 2.960(3)–3.120(4)Å for Bi-Cl(µ3). The cations and anions are held in place by weak hydrogen bonds.
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DOI: 10.1007/BF01671080
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Al-Farhan</name><affiliation wicri:level="1"><country xml:lang="fr">Arabie saoudite</country><wicri:regionArea>Department of Chemistry, College of Science, King Saud University, 11451, Riyadh</wicri:regionArea><wicri:noRegion>Riyadh</wicri:noRegion></affiliation></author><author><name sortKey="Al Wassil, Abdulaziz I" sort="Al Wassil, Abdulaziz I" uniqKey="Al Wassil A" first="Abdulaziz I." last="Al-Wassil">Abdulaziz I. Al-Wassil</name><affiliation wicri:level="1"><country xml:lang="fr">Arabie saoudite</country><wicri:regionArea>Department of Chemistry, College of Science, King Saud University, 11451, Riyadh</wicri:regionArea><wicri:noRegion>Riyadh</wicri:noRegion></affiliation></author></analytic><monogr></monogr><series><title level="j">Journal of Chemical Crystallography</title><title level="j" type="abbrev">J Chem Crystallogr</title><idno type="ISSN">1074-1542</idno><idno type="eISSN">1572-8854</idno><imprint><publisher>Kluwer Academic Publishers-Plenum Publishers</publisher><pubPlace>New York</pubPlace><date type="published" when="1995-12-01">1995-12-01</date><biblScope unit="volume">25</biblScope><biblScope unit="issue">12</biblScope><biblScope unit="page" from="841">841</biblScope><biblScope unit="page" to="844">844</biblScope></imprint><idno type="ISSN">1074-1542</idno></series></biblStruct></sourceDesc><seriesStmt><idno type="ISSN">1074-1542</idno></seriesStmt></fileDesc><profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Crystal structure</term><term>bismuth chloride complexes</term><term>diphenylammonium</term></keywords><keywords scheme="Teeft" xml:lang="en"><term>Acta</term><term>Acta crystallogr</term><term>Anion</term><term>Battaglia</term><term>Bismuth</term><term>Bismuth centers atoms</term><term>Bond angles</term><term>Bond lengths</term><term>Bond range</term><term>Cation</term><term>Chem</term><term>Chlorine atoms</term><term>Corradi</term><term>Crystal data</term><term>Crystal structure</term><term>Crystallogr</term><term>Dalton trans</term><term>Inorg</term><term>Longest bond</term><term>Trans</term></keywords></textClass><langUsage><language ident="en">en</language></langUsage></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">Abstract: [(C6H5)2NH2]4 +[Bi4Cl16]4− crystallizes in the triclinic space group $$P\bar 1$$ witha=11.835(2),b=12.393(2),c=12.625(3)Å, α=108.37(3), β=108.69(3), γ=96.00(3)° andD c=2.135 g cm−3 forZ=1. The [Bi4Cl16]4− anion is a centrosymmetric cluster of four distorted edge-sharing BiCl6 octahedra. The ranges of the Bi−Cl bonds are 2.484(4)–2.606(3)Å for Bi−Cl(terminal), 2.691(3)–2.956(4)Å for Bi-Cl(µ2), and 2.960(3)–3.120(4)Å for Bi-Cl(µ3). The cations and anions are held in place by weak hydrogen bonds.</div></front></TEI><affiliations><list><country><li>Arabie saoudite</li></country></list><tree><country name="Arabie saoudite"><noRegion><name sortKey="Al Farhan, Khalid A" sort="Al Farhan, Khalid A" uniqKey="Al Farhan K" first="Khalid A." last="Al-Farhan">Khalid A. Al-Farhan</name></noRegion><name sortKey="Al Wassil, Abdulaziz I" sort="Al Wassil, Abdulaziz I" uniqKey="Al Wassil A" first="Abdulaziz I." last="Al-Wassil">Abdulaziz I. Al-Wassil</name></country></tree></affiliations></record>Pour manipuler ce document sous Unix (Dilib)
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